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Sulphuric acid , 2.5 l

ROTIPURAN® 98 %, for nitrogen determination
Icon_EVE-EUD Please consider that this product might be liable to some legal sanctions as for example to obtain an end user declaration or the prohibition of some applications. For details please do contact your counterpart in our sales department!
Mogelijke gevolgen: vernietigen metalen en zijn bijtend voor lichaamsweefsel; ernstig oogletsel is mogelijk. Veiligheid: contact vermijden; veiligheidsbril en handschoenen dragen. Bij contact ogen en huid met water spoelen.
Danger
H290-H314
i may be corrosive to metals, causes severe skin burns and eye damage
P280 P301+P330+P331 P303+P361+P353 P305+P351+P338 P310
i wear protective gloves/protective clothing/eye protection/face protection, IF SWALLOWED: rinse mouth. Do NOT induce vomiting, IF ON SKIN (or hair): Take off immediately all contaminated clothing. Rinse skin with water [or shower], IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing, immediately call a POISON CENTER/doctor
Verwante producten
VE
Verp.
Empirical formula H2SO4
Molar mass (M) 98,08 g/mol
Density (D) 1,84 g/cm³
Boiling point (bp) 315 °C
Melting point (mp) -15 °C
ADR 8 II
WGK 1
CAS No. [7664-93-9]
EG-Nr. 231-639-5
UN-Nr. 1830

For determination of nitrogen acc. to Kjehldahl.

Guarantee analysis

62,90 €/VE 

Excl. btw | 2,5 l Per VE

Bestelnr. X945.2

Op voorraad
Vrij van verzendingskosten vanaf 125 €
Snelle en betrouwbare levering!
Vanaf 4 VE 59,76 €/VE
Vanaf 24 VE 56,61 €/VE
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Sulphuric acid
Geselecteerde hoeveelheid:   0
  1. Tussentotaal:  0.00
Bestelnr. VE Verp. Prijs Hoeveelheid
X945.1 1 l glass 31,10 €
X945.2 2,5 l glass 62,90 €
Op voorraad
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Niet beschikbaar
Leveringsdatum onbekend op dit moment
Geselecteerde hoeveelheid:   0
  1. Tussentotaal:  0.00

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Algemene informatie

Analysis of Food

Carl ROTH also offers reagents suitable for food analysis.

On the following pages, you will find the determination of
• Nitrogen according to Kjeldahl
• Sugar
• Mercury
• Trichinae
• Fat

and the determination of the
• Iodine value
• Acid value
• Peroxide value
• Saponification value

as well as other determining factors such as
• Viscosity
• Density
• Hydroxyl value
• Fluoride ions


Determination of Nitrogen according to Kjeldahl

The most common technique for measuring the amount of nitrogen in organic matter is the Kjeldahl method, which is used in a wide range of sectors such as environmental analysis, food analysis, water analysis and agricultural analysis, as well as in the pharmaceutical and chemical industries. In this traditional method, a precisely weighed sample is broken down using concentrated sulphuric acid, a process which digests its organic contents and reacts nitrogen to form ammonium sulphate.(CHNO)(s) → CO2 (g) + SO2 (g) + H2O (g) + NH4SO4 (solv, H2SO4)A catalyst or catalyst mixture consisting of copper, selenium, mercury and/or titanium is added to speed up the reaction. Sodium or potassium sulphate is used to give the sulphuric acid a higher boiling point. If the nitrogen is contained in a nitro, nitroso or azo compound, however, the mixture must be reduced with zinc before digestion takes place.
The nitrogen is now present in the sulphuric acid as ammonium sulphate. Adding a strong base (such as NaOH) neutralises the sulphuric acid and liberates ammonia from the solution.NH4SO4 (solv) + 2 NaOH (aq) → Na2SO4 (aq) + 2 NH3 (g) + 2 H2O (l) The ammonia is led into an acid (such as boric acid) by means of steam distillation.B(OH)3 (aq) + 2 H2O (l) + NH3 (g) → B(OH)4- (aq) + NH4+ (aq) The resulting strong base (borate ion) is back-titrated with a strong acid (hydrochloric acid or sulphuric acid). The excess weak boric acid is not captured in the process. A Tashiro's indicator that changes colour in the acid is used for titration. The amount of acid that has been used up can then be converted into the amount of nitrogen in the sample. NH4+ (aq) + B(OH)4- (aq) + HCl (l) → NH4Cl (aq) + B(OH)3 (aq) + H2O (l)To calculate the protein content of the sample, the varying nitrogen content of the amino acids must be checked and the relevant conversion factors applied. The nitrogen contained in food derives mainly from proteins, but different samples may also contain other sources of nitrogen.


Analysecertificaten

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Guarantee analysis

Assay (titr.)97 - 99 %  
Ash content≤0,0005 %  
Total nitrogen (N)≤0,0005 %  

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