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Acetonitrile, 4 l, glass

ROTISOLV® Pestilyse® ≥99,9 %
Mogelijke gevolgen: zijn ontvlambaar; vloeistoffen vormen met lucht explosieve mengsels; zorgen met water voor ontvlambare gassen of zijn zelfontvlambaar. Veiligheid: uit de buurt van open vuur en warmtebronnen houden; vaten dicht afsluiten; brandveilig bewaren.
Mogelijke gevolgen: leiden tot schade aan de gezondheid, irriteren organen, huid of luchtwegen. Leiden in grotere hoeveelheden tot de dood. Veiligheid: zoals hierboven; bij huidirritaties of oogcontact met water of geschikt middel spoelen.
Danger
H225-H302+H312+H332-H319
i highly flammable liquid and vapour, harmful if swallowed, in contact with skin or if inhaled, causes serious eye irritation
P210 P280 P305+P351+P338 P403+P235
i keep away from heat, hot surfaces, sparks, open flames and other ignition sources. No smoking, wear protective gloves/eye protection, IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing, store in a well-ventilated place. Keep cool
Verwante producten
VE
Verp.
Cyanomethane, Methyl cyanide
Empirical formula C2H3N
Molar mass (M) 41,05 g/mol
Density (D) 0,79 g/cm³
Boiling point (bp) 81,65 °C
Flash point (flp) 2 °C
Melting point (mp) -45,7 °C
ADR 3 II
WGK 2
CAS No. 75-05-8
EG-Nr. 200-835-2
UN-Nr. 1648

For residue and environmental analysis.

158,60 €/VE 

Excl. btw | 4 l Per VE

Bestelnr. T168.3

Op voorraad
Vrij van verzendingskosten vanaf 250 €
Snelle en betrouwbare levering!
Vanaf 6 VE 150,67 €/VE
Vanaf 24 VE 142,74 €/VE

Productdetails



Acetonitrile ROTISOLV® Pestilyse® ≥99,9 %

Technische informatie
Watermengbaarheid yes 
Acetonitrile
Geselecteerde hoeveelheid:   0
  1. Tussentotaal:  0.00
Bestelnr. VE Verp. Prijs Hoeveelheid
T168.1 2,5 l glass

105,90 €

T168.3 4 l glass

158,60 €

Op voorraad
Beschikbaar
In bestelling
Niet meer verkrijgbaar
Leveringsdatum onbekend
Geselecteerde hoeveelheid:   0
  1. Tussentotaal:  0.00

Downloads / MSDS


Algemene informatie

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ROTISOLV® Pestilyse® Solvents

for residue and environmental analysis

Field of application: ‘Pesticide Residue Analysis’ (via ECD, PND detection) in sectors environment, foodstuff, water, etc. ROTISOLV® Pestilyse® solvents are ideal as extraction agents and for sample preparation.



Eigenschappen:

  • Highest purity
  • Quality control via ECD and PND
  • Non-volatile parts: 5 ppm or less
  • Specially purified for application in pesticide residue analysis


QuEChERS Products

For pesticide residue analysis in food

The QuEChERS (Quick, Easy, Cheap, Efficient, Rugged, Safe; "Catchers") method has achieved a leading position for the determination of pesticide residues in food by GC-MS or LC-MS within a few years of its development.
This method was developed using an extraction method for pesticides in fruit and vegetables coupled with a clean-up method that removes sugars, lipids, organic acids, sterols, proteins, pigments and excess water. This technique offers a user-friendly alternative to conventional liquid-liquid and solid phase extractions.

The process involves two simple steps. First, an extraction of the homogenised samples takes place, which are split with an organic solvent and a salt solution. The supernatant is then further extracted and purified using dispersive solid phase extraction (dSPE).
This allows rapid and cost-effective processing of heavily matrix-loaded samples. In order to optimise the extraction of pH-dependent compounds, to minimise the decomposition of sensitive substances and to cover a broad matrix spectrum, various modifications of the QuEChERS method have been developed.

  • Unbuffered original method
  • European method EN 15662
  • AOAC Official 2007.01 Method
In addition to the required sorbent silica gel 60 Diamino, a number of individually weighed and premixed buffers and extraction mixtures are offered that are specially adapted to different sample matrices.

Carl ROTH offers QuEChERS extraction and dSPE products in a variety of standard sizes and formats, making the QuEChERS method even easier to use.


Extraction

The choice between the original unbuffered method salts and buffered method salts should be based on the expected pH of the final extract and the pH sensitivity of the target analytes. The unbuffered original method is well suited for most analytes. When using unbuffered salts, the pH of the final extract is largely determined by the pH of the sample. However, if critical target analytes are unstable at certain pH values, a buffered method that maintains the required pH will provide more accurate results for pH-sensitive pesticides.

For extraction, the European Standard EN 15662 recommends a citrate extraction mix, while the AOAC Standard 2007.1 uses an acetate extraction mix.


Clean up via dSPE

The key to optimising QuEChERS purification lies in the selection of absorbents that effectively remove different types of interferences in different samples. The aim is to achieve efficient but not excessive purification so that interferences are removed and the target analytes remain in the extract.
During purification, the diamino phase (PSA) removes sugars and organic acids, for example. Magnesium sulphate is used to remove water, while C18 ec removes non-polar interfering substances such as fats and the carbon phase removes pigments, sterols and other non-polar substances.
The type and relative amount of matrix components that need to be removed from the extracts prior to analysis will help you select the appropriate dSPE products.


Adsorbents and what their use

MgSO4 Removes excess of water
NaCl For phase separation
Silica Gel 60 Diamino (PSA)
(Primary Secondary Amine)
Removes organic and fatty acids, sugars and polar pigments (e.g. anthocyanes)
Silica Gel 60 C18 ec
(reversed phase modified silica)
Traps nonpolar compounds (e.g. lipids)
Carbon (GCB)
(Activated Charcoal / Graphitized Carbon Black)
Removes non polar pigments and sterols
(please note: planar pesticides are also removed)

Analysecertificaten

Hier kunt u uw analysecertificaat voor het geselecteerde product zoeken en downloaden. Geef een chargenummer op.
De volgende analysecertificaten werden gevonden:

Guarantee analysis

Assay (GC)≥99,9 %
Water (KF)≤0,2 %
Acidity≤0,0005 meq/g
Evaporation residue≤0,0005 %
GC/ECD (individual signal as lindane)≤5 ng/l
GC/PND (individual signal as ethylparathion)≤10 ng/l