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Kjeldahl tablets (Missouri catalyst), 250 unit(s)

tablet 2,5 g
H412
i harmful to aquatic life with long lasting effects
P273 P501
i avoid release to the environment, dispose of contents/container in accordance with local/regional/national/international regulations
Produkty pokrewne
Pack Qty.
Pack.
Density (D) 2,7 g/cm³
WGK 2

For determination of nitrogen.

Type analysis

96,50 €/op. 

plus VAT | 250 unit(s) za op.

Nr kat. HN22.1

Dostępny z magazynu w Karlsruhe
Szybka, prosta i niezawodna dostawa.
od 6 op. 91,68 €/op.
od 24 op. 86,85 €/op.
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Kjeldahl tablets (Missouri catalyst)
Wybrana ilość:   0
  1. Suma pośrednia:  0.00
Nr kat. Pack Qty. Pack. Cena Ilość
HN22.1 250 unit(s) plastic 96,50 €
HN22.2 1 000 unit(s) plastic 320,50 €
Dostępny z magazynu w Karlsruhe
Dostępny krótkoterminowo
Niedostępny
Data dostawy obecnie nieznana
Wybrana ilość:   0
  1. Suma pośrednia:  0.00

Pobranie


Informacje ogólne

Analysis of Food

Carl ROTH also offers reagents suitable for food analysis.

On the following pages, you will find the determination of
• Nitrogen according to Kjeldahl
• Sugar
• Mercury
• Trichinae
• Fat

and the determination of the
• Iodine value
• Acid value
• Peroxide value
• Saponification value

as well as other determining factors such as
• Viscosity
• Density
• Hydroxyl value
• Fluoride ions


Determination of Nitrogen according to Kjeldahl

The most common technique for measuring the amount of nitrogen in organic matter is the Kjeldahl method, which is used in a wide range of sectors such as environmental analysis, food analysis, water analysis and agricultural analysis, as well as in the pharmaceutical and chemical industries. In this traditional method, a precisely weighed sample is broken down using concentrated sulphuric acid, a process which digests its organic contents and reacts nitrogen to form ammonium sulphate.(CHNO)(s) → CO2 (g) + SO2 (g) + H2O (g) + NH4SO4 (solv, H2SO4)A catalyst or catalyst mixture consisting of copper, selenium, mercury and/or titanium is added to speed up the reaction. Sodium or potassium sulphate is used to give the sulphuric acid a higher boiling point. If the nitrogen is contained in a nitro, nitroso or azo compound, however, the mixture must be reduced with zinc before digestion takes place.
The nitrogen is now present in the sulphuric acid as ammonium sulphate. Adding a strong base (such as NaOH) neutralises the sulphuric acid and liberates ammonia from the solution.NH4SO4 (solv) + 2 NaOH (aq) → Na2SO4 (aq) + 2 NH3 (g) + 2 H2O (l) The ammonia is led into an acid (such as boric acid) by means of steam distillation.B(OH)3 (aq) + 2 H2O (l) + NH3 (g) → B(OH)4- (aq) + NH4+ (aq) The resulting strong base (borate ion) is back-titrated with a strong acid (hydrochloric acid or sulphuric acid). The excess weak boric acid is not captured in the process. A Tashiro's indicator that changes colour in the acid is used for titration. The amount of acid that has been used up can then be converted into the amount of nitrogen in the sample. NH4+ (aq) + B(OH)4- (aq) + HCl (l) → NH4Cl (aq) + B(OH)3 (aq) + H2O (l)To calculate the protein content of the sample, the varying nitrogen content of the amino acids must be checked and the relevant conversion factors applied. The nitrogen contained in food derives mainly from proteins, but different samples may also contain other sources of nitrogen.


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Type analysis

Appearanceblue tablets  
Composition: acc. to Missouri (K2SO4, Na2SO4 and CuSO4).

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